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Catalog No. MN701520.110
Part No. 701520.110
Supplier MACHEREY‑NAGEL
Derivatization reagents for GC, alkylation, methylation, TMSH
Net Price
Special offer
Availability

6 weeks

PROPERTIES
  • Selling unit
    1x10 mL, 5x10 mL, 10x1 mL, 20x1 mL
  • Method
    Gas chromatography (GC), derivatization
  • Composition
    Trimethylsulfonium hydroxide (TMSH) in methanol
  • Derivatization type
    Alkylation, methylation
  • Recommended application(s)
    Chlorophenols, Chlorophenoxycarboxylic acids, Derivatization, Free acids, Lipids, Phenols, Triglycerides
  • Storage temperature
    2–8 °C
  • Hazardous material
    Yes
  • Type
    Alkylation, methylation
DESCRIPTION
TMSH is used for methylation of fatty acids, because it is just necessary to add the reagent (0.2 M in methanol) to the sample solution. Removal of excess reagent is not required, since in the injector of the gas chromatograph at 250 °C pyrolysis to volatile methanol and dimethylsulfide will occur. Due to the high reactivity, complete derivatization is often obtained at ambient temperature. However, heating (e.g., 10 min at 100 °C) in a closed sample vial may be necessary. These products contain harmful substances which must be specially labeled as hazardous. For detailed information please see SDS.
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